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This research elucidated the clear presence of OPPs and estimated its ecological danger in the riverine ecosystem regarding the urbanised Linggi River, Negeri Sembilan, Malaysia. The OPP concentration in surface water was determined utilizing solid-phase extraction strategy and high-performance liquid chromatography in conjunction with diode range detection. Further, the ecological risk was expected using the risk quotient (RQ) method. The three OPPs, in