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In order to achieve proper disposal of Fenton sludge, a new recycle method for preparing adsorbents based on one-step hydrothermal carbonization synthesis of aminated hydrochar from Fenton sludge (AHFS) was developed. It was found that AHFS prepared at 340 °C for 60 min showed Pb2+ adsorption capacity as high as 359.83 mg g-1. Adsorption kinetics and thermodynamics results indicated that chemical interaction, intra-particle diffusion and monolayer homogeneous surface of AHFS dominated in adsorption process. The contribution proportion of