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The development of a novel nanobiosorbent derived from waste molasses for the adsorptive removal of arsenic (As) has been attempted in this study. Waste molasses were chemically ameliorated through a solvothermal route for the incorporation of iron oxide, thereby producing iron oxide incorporated carbonaceous nanomaterial (IOCN). Synthesis of IOCN was confirmed through transmission electron microscopy (TEM), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and atomic emission spectroscopy (AES) analysis. The surface