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MgFe-layered double hydroxides (LDHs) were prepared by co-precipitation method with the ratios of [Mg2+]/[Fe3+] varied in the range of 21-61, and occupied as heterogeneous catalysts for the degradation of Methylene Blue (M in the Fenton process. MgFe-LDH prepared with the ratio of [Mg2+]/[Fe3+] at 31 was verified to be of high purity. The Fenton-like process catalyzed by MgFe-LDH performed excellently, and more than 97% degradation of MB was obtained with 0.5 mmol/L H2O2 and 0.50 g/L MgFe-LDH at initial pH 2 at room temperature. The occ
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