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The symmetry of atomically precise nanoclusters is influenced by the specific geometry of the kernel and the arrangement of staple motifs. To understanding the role of ligand and its effect on the breaking of symmetry during ligand exchange transformation, it is necessary to have a mechanism of transformation in an atomically precise manner. Herein, we report the structural transformation from bipyramidal kernel to icosahedral kernel via ligand exchange. The transformation of [Au23(CHT)16]- to [Au25(2-NPT)18]- through ligand (aromatic)
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