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An acidified magnetic sludge-biochar (MS was prepared to enhance ammonium nitrogen (AN) removal efficiency in eutrophic water, and MSB was obtained by secondary pyrolysis of sludge biochar powder. A series of MSB were prepared under 300, 400, 500, 600 °C and different valence states of iron ions by impregnation pyrolysis, which is based on the deposition of unstable iron minerals on biochar matrix. Physicochemical properties of pristine biochar and MSB were revealed through characterization analysis, suggesting that MSB prepared b