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Transformations of nitrogen-oxyanions (NO x - ) to ammonia impart pivotal roles in sustainable biogeochemical processes . While metal mediated reductions of NO x - are relatively well known, this report herein illustrates proton-assisted activations of NO x - anions in the presence of electron rich aromatics such as 1,3,5-trimethoxybenzene (TMB - H, 1a ) leading to the formation of oxoammonium salt [(TM 2 N + =O][NO 3 - ] ( 2a ) via the intermediacy of NO + . Detailed characterizations including X-ray diffraction, multinuclear ( 1 H, 13
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