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The hydrated cement had been calcined at 900 °C, and also the hydrothermal synthesis had been completed at 220 °C for differing times. The levels for the hydrothermal products were reviewed by XRD and TG-DSC, and it had been noted that the calcination of hydrated cement impacted the formation rate of xonotlite. The information of xonotlite increased from 18per cent (synthesized with hydrated concrete without calcination) to 74per cent (synthesized from hydrated concrete with calcination