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For contrast studies, the CuO nanosphere was served by exactly the same preparation process without MWCNT. On the basis of the real characterization results, the morphological nature of CuO was seen to be a sphere-like framework, that has been embellished on the MWCNT with the average crystallite measurements of 16 nm (± 1 nm). On the basis of the electrochemical studies, the fabricated nanocomposite exhibits a wider linear number of 0.025-1375 μM,