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The aqueous-based responses had been completed at pH ~ 8, under inert environment (Ar). The reactions had been taken under differing times, and the full XRD structural evaluation was meant to evaluate the conversion from the Sn6O4(OH)4 advanced to SnO particles. Williamson-Hall analysis indicated that the scale and stress for the SnO particles had been some time course treatment centered. Microwave home heating yielded an individual tetragonal SnO phase after 1 h of thermal treatment, and TE