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Rhombohedral crystal particles of zeolitic clathrasil deca-dodecasil 3R (DDR), hydrothermally synthesized from a mixture consisting of fumed silica, water, and 1-adamantanamine, were characterized by single-crystal and powder X-ray diffractometry as a function of temperature and pole figure analysis. The crystallite was bounded by six equivalent 101̅1 faces and exhibited twin-free appearance, whereas the structure was resolved with the binary twin by merohedry, defined by the twin point group 3̅2'/m'1, consisting of two twin domains wit
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