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A hybrid catalyst of crystalline Fe2O3 with amorphous FeS was designed by a deep eutectic solvent approach with a subsequent annealing process, offering a high-efficiency electrocatalyst for N2 fixation with an NH3 yield of 34.31 μg h-1 mgcat.-1 and faradaic efficiency of 18.06% at -0.25 V versus a reversible hydrogen electrode.Circular dichroism (CD) spectroscopy is a widely-used method in biochemistry, structural biology and pharmaceutical chemistry. More than 24 000 papers published in the past decade have included CD characterisation