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This article is protected by copyright. All rights reserved. This article is protected by copyright. All rights reserved.Semiconductor oxides of bismuth and zinc have been synthesized using modified sol-gel method and sol-combustion method, respectively. The synthesized catalysts were characterized by X-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive X-rays spectroscopy (EDS), X-ray photoelectron spectroscopy (XPS) and UV-vis spectroscopy. The photocatalytic activity of Bi2 O3 and ZnO