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The major specific phenolic compounds gotten were chlorogenic acid and rutin, quantified by high-performance fluid chromatography and mess spectrometry (HPLC-MS). Zein fibers packed with 5% herb exhibited greater antioxidant task with 83.0% inhibition. The materials with various concentrations of yerba mate exhibited homogeneous morphology. Yerba mate extract encapsulated in zein fibers had greater thermal stability compared to no-cost extract. Zein fibers comprising 5% yerba ma