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Zn-MOF/ZnO nanocomposites with different organic linkers were fabricated by a rapid ultrasonication method using freshly prepared Zn(OH)2 precipitate. The high metal-to-ligand ratio led to the simultaneous formation of MOFs and ZnO nanoparticles in the MOFs. The surface area was in the range of 12-21 m2 g-1. The nanocomposites were tested for H2S adsorption at room temperature, where the maximum adsorption capacity of 14.2 mg g-1 was recorded for ZnBTC/ZnO in dry conditions. The spent adsorbents were regenerated using methanol and UV ir