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Electrokinetic plus in situ UV-Vis spectroscopic analyses declare that redox energetic nickel hydroxide types is made on the surface of NiO electrocatalysts during HMF oxidation, and also this Ni(II) hydroxide oxidation to Ni(III) oxyhydroxide action may be the price determining step (RDS). This mechanistic study for biomass oxidation in CO2-saturated electrolyte provides insight into constructing an extremely efficient system for the paired electrolysis of CO2 reductio
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