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Both Fe(III) and fatty acids are ubiquitous and important species in environmental waters. Because they are amphipathic, many fatty acids are surface active and prone to enrichment at the air-water interface. Here, we report that by using nonanoic acid (NA) as a model fatty acid, coexisting Fe(III), even at concentrations as low as 1 μM, markedly enhanced the photochemical release of NA-derived volatile organic compounds (VOCs) such as octanal and octane into the air. Further studies indicated that the surface-enriched fatty acids drama