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Bulk GaPO4 is an advanced piezoelectric material operating under large temperatures based on the α-β period transition at 970 °C. This work provides the technological improvement a hydrothermal refluxing method initially sent applications for GaPO4 solitary crystal development. Crystals of 10-20 g had been grown in mixtures of aqueous solutions of reasonable- and high-vapor-pressure acids (H3PO4/HCl) at 180-240 °C (10-20 bars)
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