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This work illustrates the power of combining abiological biocatalysis with chemoenzymatic synthesis for generating collections of optically active scaffolds of high value for medicinal chemistry and drug discovery.The controllable construction and function expansion of some sophisticated aggregations represent a current hot topic in scientific research. In this paper, using a prefabricated Co14 cluster as a synthetic precursor, a homometallic Co24 and a heterometallic Co12Cd12 giant cluster possessing similar dual-[M12] (M = Co/Cd) skel
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