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Phthalate esters (PAEs) are a class of the emerging pollutants that pose a potential environmental threat to marine ecosystems. In this study, a simple analytical method using ultrasound-assisted extraction combined with gas purges microsyringe extraction (GP-MSE) coupled with GC-MS was utilized for the reliable and rapid determination of PAEs in different types of marine sediment. The analytical results showed that the method exhibited excellent reproducibility, linear responses, and detection limits, which verified the suitability of