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Thermal pretreatment is a shared method to improve the efficiency of straw biochemical conversion. However, the process is often accompanied by problems such as the loss of carbon source. The objective of this study was to develop a novel thermal pretreatment method, called air frying, with less loss of biodegradable organic matter and favorable surface hydrophilicity. After pretreatment of two straws, the sugar yields were improved, and the improvement effect of corn stover was more significant. The total saccharification rate of cor