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Orthorhombic β-LiScGe2O6 single crystals were compressed hydrostatically up to 10.35 GPa using a diamond anvil cell and investigated in situ by means of X-ray diffraction and Raman spectroscopy. Crystal-structure investigations at ambient conditions and at high pressure show a structural transition from an orthopyroxene-type Pbca structure (a ≈ 18.43 Å, b ≈ 8.85 Å, and c ≈ 5.34 Å at 8.6 ± 0.1 GPa) to a postorthopyroxene type P21/c structure of the new dense γ-LiScGe2O6 (a ≈ 18.62 Å, b ≈ 8.85 Å, c ≈ 5.20 Å, and β ≈ 93.1° at 9.5 ± 0.1 GPa).
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