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© 2020 John Wiley Sons A/S. Published by John Wiley Sons Ltd.The asymmetric polyethersulfone (PES-15 wt.%) mixed matrix membranes were prepared by incorporation of carbon molecular sieve (CMS) with varying concentrations (1, 3, 5 wt.%). Physico-chemical characterization of synthesized membranes was carried out using field emission scanning electron microscope, atomic force microscopy, contact angle, thermogravimetric analysis, zeta potential analyzer, porosity, and mean pore sizes. Performance analysis of synthesized mixed m