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This is due to the improved physical interactions between the GTR/NBR matrix and highly dispersive silica when using peroxide systems. It was confirmed using the analysis of the Wolff activity coefficient, indicating the enhanced synergy.Electrospinning is a flexible polymer processing method to produce nanofibres, which can be applied in the biomedical field. The current study aims to develop new electrospun hybrid nanocomposite systems to benefit the sustained release of hydrophilic drugs with hydrophobic polymers. In particular, electro