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Nanophotocatalyst MnTiO3 powders were synthesized by sol-gel technique and characterized by means of X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), as well as their thermal behavior has been studied by differential thermal and thermogravimetric analyses (DTA/TGA). Powders morphology was analyzed by means of Transmission electron microscopy (TEM). Effect of various process parameters like amount of photocatalyst, dye concentration, solution pH and irradiation time on the extent of removal of dye were studied in