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In this study, an innovative magnetic demulsifier (MD) was prepared by grafting a silica layer onto the surface of the Fe3O4 magnetic nanoparticles (MNPs) using the modified Stober process. The MD was characterized using various analytical techniques (XRD, FTIR, TGA, TEM, VSM, etc.) and employed to recover oil from O/W emulsion, which were then regenerated and recycled several times. The effects of magnetic demulsifier dosage (MDdose), the concentration of oil (Coil), pH, the concentration of the surfactant (Csur), and separation time (t
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