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Digestates, a byproduct of the anaerobic bioconversion of organic wastes for the production of biogas, are highly variable in chemical and biological properties, thus limiting their potential use in agriculture as soil amendment. Using a lab-scale glass reactor, we aimed to assess the feasibility to chemically stabilize the solid fraction of an anaerobic digestate by applying a Fenton reaction under constant pH (3., temperature (70 °C), reaction time (8 h), and various combinations of H2O2 and Fe2+. In Fenton-treated samples, the phyt